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Electron Microscopy and XPS (ESCA)


MCLinc staff includes specialists are specialized in electron microscopy.  Five electron microscopes provide MCLinc scientists with powerful tools for materials analysis, corrosion studies, particulate speciation, source profiling, forensic investigations, and a host of additional applications.

The X-ray Photoelectron Spectrometer (XPS) provides surface analysis at 20 to 40 Angstrom units depth.  XPS can be used for identification of compounds, determination of oxidation states of constituents, chemical speciation, and depth profiling.


Three scanning electron microscopes (SEM) and one transmission electron microscope (TEM) provide ultra high-resolution microscopy (magnification to 1,000,000x) to identify extremely small particles.  All are equipped with energy dispersive x-ray spectroscopy (EDS) to provide elemental analysis.


The ESEM (environmental scanning electron microscope) is a unique SEM instrument that allows the sample to be subjected to low-pressure gas conditions (water vapor and other gases) at pressures up to 15 torr.  This allows the observation of reactions between a substrate or its corrosion products with water vapor or selected gases.

 


Materials and Chemistry Laboratory, Inc.
East Tennessee Technology Park, Bldg. K-1006 • Oak Ridge, TN 37830-1702
Voice: (865) 576-4138 • FAX: (865) 576-8558
Contact:
Barry A. Stephenson
, President

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